Title
Utilization of standards generated in the process of thermal decomposition chemically modified silica gel for a single point calibration of a GC/FID system
Document Type
Article
Publication Date
4-2-1998
Publication Title
Talanta
Abstract
The utilization of a multicomponent gaseous standard mixture, containing CO and CO(2) and obtained by thermal decomposition of a so-called immobilized compound, for a single point calibration of a GC/FID system are described. The generation of such a mixture takes place as a result of thermal decomposition of a sample of chemically modified silica gel placed in a heated chamber of thermal desorber coupled with the device being calibrated via a catalytic methanizer. The mean amount of the analyte librated from unit mass of the gel was 0.71 mg g(-1) (RSD = 3%) for carbon monoxide and 0.86 mg g(-1) (RSD = 3%) for carbon dioxide.
Volume
44
Issue
9
First Page
1551
Last Page
1561
DOI
https://doi.org/10.1016/S0039-9140(96)02177-7
ISSN
0039-9140
Rights
© 1997 Published by Elsevier B.V.
Recommended Citation
Prokopowicz, Magdalena; Luboch, Elzbieta; Namiesnik, Jacek; Biernat, Jan F.; and Przyjazny, Andrzej, "Utilization of standards generated in the process of thermal decomposition chemically modified silica gel for a single point calibration of a GC/FID system" (1998). Chemistry & Biochemistry Publications. 11.
https://digitalcommons.kettering.edu/chem_biochem_facultypubs/11
Comments
ESSN: 1873-3573